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Applications / edited by Ferenc Darvas, Volker Hessel, György Dorman

By: Contributor(s): Resource type: Ressourcentyp: Buch (Online)Book (Online)Language: English Series: De Gruyter Textbook | Flow Chemistry ; Volume 2Publisher: Berlin/Boston : De Gruyter, 2014Copyright date: ©2014Description: Online-Ressource (350 p)ISBN:
  • 9783110367508
Subject(s): Additional physical formats: 9783110367072 | Erscheint auch als: Flow chemistry ; Volume 2: Applications. Druck-Ausgabe. Berlin : De Gruyter, 2014. xx, 329 SeitenDDC classification:
  • 543/.22
LOC classification:
  • TP156.F6
  • TP156.F6 D373 2014
DOI: DOI: 10.1515/9783110367508Online resources:
Contents:
Preface; About the editors; Contributing authors; Abbreviations; Part I Catalysis and activation Clemens Brechtelsbauer and King Kuok (Mimi) Hii; 1. Catalysis in flow; 1.1 Introduction; 1.1.1 Flow versus batch chemistry; 1.1.2 Development of catalytic reactions and flow for organic synthesis; 1.2 Reactor types, catalytic reactions and productivity; 1.2.1 Solid-liquid reactors; 1.2.2 Solid-liquid-gas systems; 1.3 Conclusion; 2 Catalytic engineering aspects of flow chemistry; 2.1 Introduction; 2.2 Basis of (catalytic) reactor engineering; 2.2.1 Flow motion in reactors; 2.2.2 Relevant physics
2.2.3 Characteristic times2.2.4 Characteristic lengths; 2.2.5 Surface area; 2.2.6 Mixing; 2.2.7 Heat issues; 2.3 Describing the chemistry; 2.3.1 Kinetic rate laws; 2.3.2 Rate measurement and reaction time; 2.3.3 Catalyst deactivation; 2.4 Methodology for Flow reactor dimensioning; 2.4.1 Batch versus Flow reactor comparison; 2.4.2 Checking for mass and heat transfer limitations; 2.4.3 Basis for reactor scale-up; 2.5 Conclusion; 3 Continuous-flow photochemistry in microstructured environment; 3.1 Environmental impact in view of Green Chemistry
3.2 Physical considerations - reasons why microstructured equipment is preferred for flow photochemistry3.2.1 Absorption of light by molecules in solution; 3.2.2 Role of solvent; 3.2.3 Micrometer-sized structures as key elements of reactor equipment for flow photochemistry; 3.3 Technological considerations for flow photochemistry; 3.3.1 Light sources; 3.3.2 Reactor concepts for flow photochemistry; 3.4 Chemical considerations for flow photochemistry; 3.4.1 Photochemical reactions without catalyst material; 3.4.2 Heterogeneous flow photocatalysis
3.4.3 Flow photocatalysis with organic dyes or noble metal complexes3.5 Summary and outlook; 4 Electrochemistry in flow; 4.1 Introduction; 4.2 Electrochemistry in flow; 4.3 Microreactor design; 4.3.1 Thin gap cells; 4.3.2 ELMI - microstructured high pressure single pass thin gap flow cell; 4.3.3 Segmented thin gap flow cells; 4.4 Electrochemistry in microreactors; 4.4.1 Direct product synthesis; 4.4.2 Electrolyte free synthesis; 4.4.3 Activation of chemicals; 4.5 Ionic liquids in electrochemistry; Part II Cutting-edge applications in advanced and functional materials
5 Synthesis of materials in flow - principles and practice5.1 Introduction; 5.2 Unique properties of microreactors; 5.2.1 Mixing; 5.2.2 Thermal and pressure control; 5.2.3 Fluid behavior; 5.3 Synthesis of materials in flow; 5.3.1 Linear polymers; 5.3.2 Beads, disks, and other solid polymeric materials; 5.3.3 Janus materials; 5.3.4 Capsules; 5.3.5 Membranes and fibers; 5.3.6 Nanoparticles and inorganic nonpolymeric materials; 5.4 Conclusions; 6 Flow chemistry for nanotechnology; 6.1 Introduction to nanotechnology and graphene technology; 6.1.1 Introduction; 6.1.2 Definition and concepts
6.1.3 Brief history of nanotechnology
Summary: The emerging concept of flow chemistry promotes the transformation of present day's organic processes into a more rapid continuous set of synthesis operations, more compatible with the envisioned sustainable world. In this book, an international team of authors from academia and industry presents practical aspects. Ferenc Darvas, Florida International University, USA; György Dorman, ThalesNano, Hungary; Volker Hessel, TU Eindhoven, The Netherlands.Original version: Originalfassung: 2014PPN: PPN: 1658679598Package identifier: Produktsigel: ZDB-23-GBA | ZDB-23-GPS | EBA-BACKALL | EBA-CL-CHCOMSGSEN | EBA-DGALL | EBA-EBACKALL | EBA-EBKALL | EBA-ECL-CHCOMSGSEN | EBA-EEBKALL | EBA-ESTMALL | EBA-STMALL | ZDB-23-GBA | ZDB-23-GPS | GBV-deGruyter-alles | ZDB-23-DCM | ZDB-23-DGG | BSZ-23-EBA-C1UB | EBA-ESTMALL2 | EBA-EXCL | EBA-EBKALL2 | EBA-EEBKALL2 | EBA-STMALL2
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