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Comprehensive chromatography in combination with mass spectrometry / edited by Luigi Mondello
Mitwirkende(r): Resource type: Ressourcentyp: Buch (Online)Buch (Online)Sprache: Englisch Reihen: Wiley-Interscience series on mass spectrometryVerlag: Hoboken, N.J : Wiley, c2011Auflage: Online-AusgBeschreibung: Online-Ressource (1 online resource (xii, 481 p.)) : ill. (chiefly col.)ISBN:- 9781283203760
- 1283203766
- 9781118003442
- 543.8
- QD79.C4
Inhalte:
Zusammenfassung: Intro -- Comprehensive Chromatography in Combination with Mass Spectrometry -- Contents -- Contributors -- Preface -- 1. Introduction -- 1.1 Two-Dimensional Chromatography-Mass Spectrometry: A 50-Year-Old Combination -- 1.2 Shortcomings of One-Dimensional Chromatography -- 1.3 Benefits of Two-Dimensional Chromatography -- 1.4 Book Content -- 1.5 Final Considerations -- 2. Multidimensional Gas Chromatography: Theoretical Considerations -- 2.1 Symbols -- 2.2 One-Dimensional GC -- 2.3 Comprehensive GC x GC -- 3. Multidimensional Liquid Chromatography: Theoretical Considerations -- 3.1 Two-Dimensional LC Techniques -- 3.2 Peak Capacity in HPLC: One- and Multidimensional Separations -- 3.3 Orthogonality in Two-Dimensional LC-LC Systems -- 3.4 Sample Dimensionality and Structural Correlations -- 3.5 Separation Selectivity and Selection of Phase Systems in Two-Dimensional LC-LC -- 3.6 Programmed Elution in Two-Dimensional HPLC -- 3.7 Fraction Transfer Modulation in Comprehensive LC x LC: Additional Band Broadening -- 3.8 Future Perspectives -- 4. History, Evolution, and Optimization Aspects of Comprehensive Two-Dimensional Gas Chromatography -- 4.1 Fundamentals of GC x GC -- 4.2 Modulation -- 4.3 GC x GC Data Interpretation -- 4.4 GC x GC Instrumentation -- 4.5 Thermal Modulators -- 4.6 Comprehensive Two-Dimensional GC Method Optimization -- 4.7 Final Remarks -- 5. Flow-Modulated Comprehensive Two-Dimensional Gas Chromatography -- 5.1 Timing Requirements of GC x GC Modulators -- 5.2 Criteria for Evaluating Modulators -- 5.3 Forms of Modulation -- 5.4 Single-Stage Flow Modulation -- 5.5 Two-Stage Flow Modulation -- 5.6 Summary of Flow Modulators -- 5.7 Brief Comparison to Thermal Modulation -- 5.8 Concluding Remarks -- 6. Comprehensive Two-Dimensional Gas Chromatography Combined with Mass Spectrometry -- 6.1 Instrument Requirements for GC x GC-MS.PPN: PPN: 80937188XPackage identifier: Produktsigel: ZDB-26-MYL | ZDB-30-PAD | ZDB-30-PQE
""Series Page""; ""Title Page""; ""Copyright""; ""Contributors""; ""Preface""; ""Chapter 1: Introduction""; ""1.1 Two-dimensional chromatographyâ€"mass spectrometry: a 50-year-old combination""; ""1.2 Shortcomings of one-dimensional chromatography""; ""1.3 Benefits of two-dimensional chromatography""; ""1.4 Book content""; ""1.5 Final considerations""; ""References""; ""Chapter 2: Multidimensional Gas Chromatography: Theoretical Considerations""; ""2.1 Symbols""; ""2.2 One-Dimensional GC""; ""2.3 Comprehensive GC Ã- GC""; ""References""
""Chapter 3: Multidimensional Liquid Chromatography: theoretical considerations""""3.1 Two-dimensional LC techniques""; ""3.2 Peak capacity in HPLC: one- and multidimensional separations""; ""3.3 Orthogonality in two-dimensional LCâ€"LC systems""; ""3.4 Sample dimensionality and structural correlations""; ""3.5 Separation selectivity and selection of phase systems in two-dimensional LCâ€"LC""; ""3.6 Programmed elution in two-dimensional HPLC""; ""3.7 Fraction transfer modulation in comprehensive LC Ã- LC: additional band broadening""; ""3.8 Future perspectives""
""Chapter 4: History, Evolution, and Optimization Aspects of Comprehensive Two-Dimensional Gas Chromatography""""4.1 Fundamentals of GC Ã- GC""; ""4.2 Modulation""; ""4.3 GC Ã- GC Data Interpretation""; ""4.4 GC Ã- GC Instrumentation""; ""4.5 Thermal modulators""; ""4.6 Comprehensive Two-Dimensional GC Method Optimization""; ""4.7 Final Remarks""; ""References""; ""Chapter 5: Flow-Modulated Comprehensive Two-Dimensional Gas Chromatography""; ""5.1 Timing Requirements of GC Ã- GC Modulators""; ""5.2 Criteria for Evaluating Modulators""; ""5.3 Forms of Modulation""
""5.4 Single-Stage Flow Modulation""""5.5 Two-Stage Flow Modulation""; ""5.6 Summary of Flow Modulators""; ""5.7 Brief Comparison to Thermal Modulation""; ""5.8 Concluding Remarks""; ""References""; ""Chapter 6: Comprehensive two-dimensional gas chromatography combined with mass spectrometry""; ""6.1 Instrument requirements for GC Ã- GCâ€"MS""; ""6.2 Data processing of GC Ã- GCâ€"TOF MS results""; ""6.3 Method translation in GC Ã- GCâ€"MS""; ""6.4 GC Ã- MS""; ""6.5 Conventional and alternative modulation techniques for GC Ã- GCâ€"MS""; ""6.6 GC Ã- GCâ€"MS APPLICATIONS""
""6.7 Concluding remarks""""References and Further Reading""; ""Chapter 7: Detector Technologies and Applications in Comprehensive Two-dimensional Gas Chromatography""; ""7.1 Detection in GC Ã- GC""; ""7.2 Comments on GC Ã- GC with Mass Spectrometry""; ""7.3 Flame Ionization Detection in GC Ã- GC""; ""7.4 Electron Capture Detection in GC Ã- GC""; ""7.5 Sulfur Chemiluminescence Detection in GC Ã- GC""; ""7.6 Nitrogen Chemiluminescence Detection in GC Ã- GC""; ""7.7 Atomic Emission Detection in GC Ã- GC""; ""7.8 Thermionic Detection in GC Ã- GC""; ""7.9 Flame Photometric Detection in GC Ã- GC""
""7.10 Case Study of GC Ã- GC with selective detection""
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